1GWE
Atomic resolution structure of Micrococcus Lysodeikticus catalase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7B |
| Temperature [K] | 110 |
| Detector technology | IMAGE PLATE |
| Collection date | 1996-12-15 |
| Detector | MARRESEARCH |
| Spacegroup name | P 42 21 2 |
| Unit cell lengths | 105.785, 105.785, 105.001 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 74.540 - 0.880 |
| R-factor | 0.089 |
| Rwork | 0.089 |
| R-free | 0.09600 |
| Structure solution method | OTHER |
| RMSD bond length | 0.016 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.1.11) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 74.536 | 0.890 |
| High resolution limit [Å] | 0.882 | 0.880 |
| Rmerge | 0.048 | 0.275 |
| Number of reflections | 457407 | |
| <I/σ(I)> | 24.4 | 3.44 |
| Completeness [%] | 99.2 | 88.8 |
| Redundancy | 7.4 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.2 | pH 5.20 |
