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1GSD

GLUTATHIONE TRANSFERASE A1-1 IN UNLIGANDED FORM

Experimental procedure
Source typeSYNCHROTRON
Source detailsEMBL/DESY, HAMBURG BEAMLINE X31
Synchrotron siteEMBL/DESY, HAMBURG
BeamlineX31
Collection date1993-09-15
DetectorMARRESEARCH
Wavelength(s)0.92
Spacegroup nameC 1 2 1
Unit cell lengths100.200, 94.800, 104.000
Unit cell angles90.00, 92.50, 90.00
Refinement procedure
Resolution7.500 - 2.500
R-factor0.238
Rwork0.238
R-free0.26400
RMSD bond length0.010
RMSD bond angle1.430
Data reduction softwareDENZO
Phasing softwareX-PLOR
Refinement softwareX-PLOR
Data quality characteristics
 Overall
Low resolution limit [Å]20.000
High resolution limit [Å]2.500
Rmerge0.107
Total number of observations72511

*

Number of reflections31802
Completeness [%]97.5
Redundancy2.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion

*

20

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein55 (mg/ml)
21dropPEG200010-20 (%)
31dropTris-HCl100 (mM)
41dropNaAc30 (mM)
51dropbeta-mercaptoethanol1 (%)
61reservoirPEG200010-20 (%)
71reservoirTris-HCl100 (mM)
81reservoirNaAc30 (mM)
91reservoirbeta-mercaptoethanol1 (%)

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