1GMV
Structure of UreE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Temperature [K] | 100 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.114, 80.415, 99.848 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 17.000 - 2.800 |
R-factor | 0.2369 |
Rwork | 0.237 |
R-free | 0.31790 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.278 |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 17.000 |
High resolution limit [Å] | 2.800 |
Rmerge | 0.087 |
Number of reflections | 8277 |
Completeness [%] | 98.5 |
Redundancy | 9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.50 |