1GMU
Structure of UreE
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Temperature [K] | 100 |
Wavelength(s) | 1.0500, 0.9500, 0.9815, 0.9805 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.882, 129.360, 56.786 |
Unit cell angles | 90.00, 93.72, 90.00 |
Refinement procedure
Resolution | 17.000 - 1.500 |
R-factor | 0.223 |
Rwork | 0.223 |
R-free | 0.26100 |
Structure solution method | MAD |
RMSD bond length | 0.005 |
RMSD bond angle | 1.302 |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 17.000 |
High resolution limit [Å] | 1.500 |
Rmerge | 0.026 |
Number of reflections | 97562 |
Completeness [%] | 96.9 |
Redundancy | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.50 |