1GMH

REFINED CRYSTAL STRUCTURE OF "AGED" AND "NON-AGED" ORGANOPHOSPHORYL CONJUGATES OF GAMMA-CHYMOTRYPSIN

Experimental procedure

Spacegroup name	P 42 21 2
Unit cell lengths	69.900, 69.900, 96.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.100
R-factor	0.187
RMSD bond length	0.016
RMSD bond angle	0.027
Refinement software	PROLSQ (1GMH)

Data quality characteristics

	Overall
High resolution limit [Å]	2.100 *
Rmerge	0.068 *
Number of reflections	11120 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	5.5 *		Cohen, G.H., (1981) J. Mol. Biol., 148, 449. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	12.5 (mg/ml)
2	1	1	ammonium sulfate	50 (%sat)