1GK7
HUMAN VIMENTIN COIL 1A FRAGMENT (1A)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1999-04-15 |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 56.770, 56.770, 58.420 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.390 - 1.400 |
R-factor | 0.198 |
Rwork | 0.197 |
R-free | 0.21600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zta |
RMSD bond length | 0.020 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CCP4 |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.450 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.037 | 0.560 |
Number of reflections | 11440 | |
<I/σ(I)> | 17 | 1.9 |
Completeness [%] | 99.7 | 99.6 |
Redundancy | 10.3 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 2.0M AMMONIUM ACETATE, 10%(V/V) DIOXANE, 0.1M MES/NA, PH6.5, pH 6.50 |