1GIC
CONCANAVALIN A COMPLEXED WITH METHYL ALPHA-D-GLUCOPYRANOSIDE
Experimental procedure
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 293 |
Detector technology | AREA DETECTOR |
Collection date | 1988 |
Detector | SIEMENS |
Spacegroup name | I 21 3 |
Unit cell lengths | 167.800, 167.800, 167.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 100.000 - 2.000 |
R-factor | 0.17 |
Rwork | 0.170 |
Structure solution method | MIR + MR |
Starting model (for MR) | 1con |
RMSD bond length | 0.014 |
RMSD bond angle | 3.200 |
Data reduction software | XENGEN ((TO 5.2A)) |
Data scaling software | CCP4 ((AGROVATA) |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Rmerge | 0.046 |
Number of reflections | 34648 |
Completeness [%] | 64.0 |
Redundancy | 30 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | dialysis | 6.8 | DIALYSIS; 5MM PROTEIN CONCENTRATION WITH, pH 6.8, dialysis |