1GHF

ANTI-ANTI-IDIOTYPE GH1002 FAB FRAGMENT

Experimental procedure

Detector technology	AREA DETECTOR
Detector	XUONG-HAMLIN MULTIWIRE
Spacegroup name	P 4 21 2
Unit cell lengths	150.400, 150.400, 43.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 2.700
R-factor	0.21
Rwork	0.210
RMSD bond length	0.017
RMSD bond angle	28.700 *
Data reduction software	XENGEN ((HOWARD)
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.700 *	2.700 *
Rmerge	0.076
Total number of observations	65132 *
Number of reflections	13743
Completeness [%]	97.0	92 *
Redundancy	4.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	5 (mg/ml)
2	1	drop	PEG3350	6 (%(w/v))
3	1	reservoir	PEG3350	12 (%)