1GGB

MAJOR ANTIGEN-INDUCED DOMAIN REARRANGEMENTS IN AN ANTIBODY

Experimental procedure

Spacegroup name	I 2 2 2
Unit cell lengths	123.100, 119.500, 109.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 * - 2.800
R-factor	0.2
Rwork	0.200
RMSD bond length	0.020
RMSD bond angle	3.900
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.600 *
Rmerge	0.121 *
Completeness [%]	88.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	7 *		referred to 'Stura, E.A.', (1992) 'Proteins.Struct.,Funct., Genet.', 14, 499-508 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	Fab	8 (mg/ml)
2	1	reservoir		1.8 (M)