1GFN
OMPF PORIN DELETION (MUTANT DELTA 109-114)
Experimental procedure
Detector technology | DIFFRACTOMETER |
Collection date | 1993-12-09 |
Detector | ENRAF-NONIUS FAST |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 117.700, 117.700, 52.700 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 3.100 |
R-factor | 0.188 * |
Rwork | 0.190 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.705 |
Data reduction software | MADNES |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 3.100 * |
Rmerge | 0.090 |
Number of reflections | 7211 |
Completeness [%] | 97.8 |
Redundancy | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | 10 (mg/ml) | |
2 | 1 | 2 | PEG2000 | 10.5 (%) |