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1GAK

CRYSTAL STRUCTURE OF GREEN ABALONE SP18

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL9-1
Synchrotron siteSSRL
BeamlineBL9-1
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date1997-06-14
DetectorMARRESEARCH
Wavelength(s)0.77
Spacegroup nameP 65
Unit cell lengths68.760, 68.760, 67.710
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution60.000 - 1.850
R-factor0.227

*

Rwork0.227
R-free0.24730
Structure solution methodMIR
RMSD bond length0.010
RMSD bond angle1.242
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareSHARP
Refinement softwareCNS (0.9)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]59.7601.900
High resolution limit [Å]1.8501.850
Rmerge0.0680.311
Total number of observations82274

*

Number of reflections15134
<I/σ(I)>82.4
Completeness [%]98.998.9
Redundancy5.44
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP4.9

*

22

*

mPEG 5000, Ammonium Acetate, Sodium Phosphate, pH 3, VAPOR DIFFUSION, SITTING DROP, temperature 298K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropsodium acetate50 (mM)
21dropprotein10 (mg/ml)
31reservoirmPEG500025 (%)
41reservoirammonium acetate200 (mM)
51reservoirsodium phosphate100 (mM)

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