1GAK
CRYSTAL STRUCTURE OF GREEN ABALONE SP18
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1997-06-14 |
Detector | MARRESEARCH |
Wavelength(s) | 0.77 |
Spacegroup name | P 65 |
Unit cell lengths | 68.760, 68.760, 67.710 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 60.000 - 1.850 |
R-factor | 0.227 * |
Rwork | 0.227 |
R-free | 0.24730 |
Structure solution method | MIR |
RMSD bond length | 0.010 |
RMSD bond angle | 1.242 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | CNS (0.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.760 | 1.900 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.068 | 0.311 |
Total number of observations | 82274 * | |
Number of reflections | 15134 | |
<I/σ(I)> | 8 | 2.4 |
Completeness [%] | 98.9 | 98.9 |
Redundancy | 5.4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.9 * | 22 * | mPEG 5000, Ammonium Acetate, Sodium Phosphate, pH 3, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | sodium acetate | 50 (mM) | |
2 | 1 | drop | protein | 10 (mg/ml) | |
3 | 1 | reservoir | mPEG5000 | 25 (%) | |
4 | 1 | reservoir | ammonium acetate | 200 (mM) | |
5 | 1 | reservoir | sodium phosphate | 100 (mM) |