Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1G79

X-RAY STRUCTURE OF ESCHERICHIA COLI PYRIDOXINE 5'-PHOSPHATE OXIDASE COMPLEXED WITH PYRIDOXAL 5'-PHOSPHATE AT 2.0 A RESOLUTION

Experimental procedure
Experimental methodLAUE
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]98
Detector technologyIMAGE PLATE
Collection date2000-03-24
DetectorRIGAKU RAXIS II
Wavelength(s)1.5418
Spacegroup nameP 31 2 1
Unit cell lengths63.720, 63.720, 124.360
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution55.000 - 2.000
R-factor0.2114
Rwork0.208
R-free0.22400
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)1dnl
RMSD bond length0.012
RMSD bond angle22.900

*

Data reduction softwarebioteX
Data scaling softwarebioteX
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]55.0002.100
High resolution limit [Å]2.0002.000
Rmerge0.0560.251
Total number of observations71938

*

Number of reflections202022659

*

<I/σ(I)>12.33.3
Completeness [%]98.197.7
Redundancy3.53.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.2

*

298macroseeding

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirammonium sulfate0.8-1.1 (M)
21reservoirMES-NaOH0.1 (M)
31reservoirdioxane5 (%)

217705

PDB entries from 2024-03-27

PDB statisticsPDBj update infoContact PDBjnumon