1G6T
STRUCTURE OF EPSP SYNTHASE LIGANDED WITH SHIKIMATE-3-PHOSPHATE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 2000-03-29 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.035, 84.936, 87.624 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.940 - 1.600 |
R-factor | 0.155 |
Rwork | 0.155 |
R-free | 0.18500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.800 |
Data scaling software | XDS |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.650 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.049 | 0.181 * |
Total number of observations | 182207 * | |
Number of reflections | 57076 | 4837 * |
<I/σ(I)> | 15.1 | 4.7 |
Completeness [%] | 98.6 | 95.7 |
Redundancy | 3.3 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7 | 20 * | pH 7, VAPOR DIFFUSION, temperature 293K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | sodium formate | 1 (M) | |
2 | 1 | reservoir | sodium potassium phosphate | 25 (mM) | pH7. |
3 | 1 | drop | S3P | 5 (mM) |