1G3T
CYS102SER DTXR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-12-15 |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 63.000, 63.000, 216.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.350 |
Rwork | 0.238 |
R-free | 0.31800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.700 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.000 | 2.430 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.053 | 0.360 |
Number of reflections | 19654 | |
<I/σ(I)> | 15.6 | |
Completeness [%] | 90.5 | 56 |
Redundancy | 3.9 | 1.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 298 | Ammonium sulfate, glycerol, EDTA, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |