1FXR
CRYSTAL STRUCTURE OF THE FERREDOXIN I FROM DESULFOVIBRIO AFRICANUS AT 2.3 ANGSTROMS RESOLUTION
Experimental procedure
Spacegroup name | P 21 21 2 |
Unit cell lengths | 96.600, 58.100, 20.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.300 |
R-factor | 0.182 |
Rwork | 0.182 |
R-free | 0.22700 |
RMSD bond length | 0.013 |
RMSD bond angle | 2.930 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.500 * |
Rmerge | 0.086 * |
Completeness [%] | 70.6 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 26.6 (mg/ml) | |
2 | 1 | reservoir | ammonium sulfate | 53-65 (%sat) | |
3 | 1 | reservoir | sodium acetate | 0.1 (M) |