1FXI
STRUCTURE OF THE [2FE-2S] FERREDOXIN I FROM THE BLUE-GREEN ALGA APHANOTHECE SACRUM AT 2.2 ANGSTROMS RESOLUTION
Experimental procedure
Spacegroup name | P 41 |
Unit cell lengths | 92.200, 92.200, 47.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.200 |
R-factor | 0.23 |
RMSD bond length | 0.019 |
RMSD bond angle | 0.074 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Total number of observations | 42249 * |
Number of reflections | 21790 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * | 4 * | Kunita, A., (1978) J.Biochem.(Tokyo), 84, 989. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein solution | 1-3 (%) | |
2 | 1 | 2 | ammonium sulfate | 75 (%sat) | |
3 | 1 | 2 | 0.7 (M) | ||
4 | 1 | 2 | Tris-HCl | 0.1 (M) |