1FVX
CLOSTRIDIUM BEIJERINCKII FLAVODOXIN MUTANT: G57N OXIDIZED
Experimental procedure
| Temperature [K] | 277 |
| Detector technology | AREA DETECTOR |
| Collection date | 1990-06 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 61.520, 61.520, 70.770 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 1.900 |
| R-factor | 0.176 |
| Rwork | 0.176 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 23.090 * |
| Data reduction software | SDMS (DETECTOR SYSTEM (NIELSEN)) |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 |
| High resolution limit [Å] | 1.900 |
| Rmerge | 0.060 * |
| Number of reflections | 12436 |
| Completeness [%] | 99.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 6.8 * | 4 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | ammonium sulfate | 2.5-2.8 (M) | |
| 2 | 1 | reservoir | Tris-HCl | or phosphate |
