1FUU
YEAST INITIATION FACTOR 4A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL1-5 |
Synchrotron site | SSRL |
Beamline | BL1-5 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-07-20 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 1 |
Unit cell lengths | 38.800, 71.200, 73.200 |
Unit cell angles | 94.00, 89.60, 101.00 |
Refinement procedure
Resolution | 40.000 - 2.500 |
R-factor | 0.252 |
Rwork | 0.243 |
R-free | 0.27300 * |
RMSD bond length | 0.007 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.071 * | 0.097 * |
Total number of observations | 53337 * | |
Number of reflections | 16117 | |
Completeness [%] | 92.0 * | 80.4 * |
Redundancy | 2.99 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.5 * | 298 | CHAPS, guanidinium, KOAc, pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | mPEG550 | 20 (%) | |
2 | 1 | 1 | 1 (mM) | ||
3 | 1 | 1 | MES | 100 (mM) |