1FUQ
FUMARASE WITH BOUND 3-TRIMETHYLSILYLSUCCINIC ACID
Experimental procedure
Temperature [K] | 294 |
Detector technology | AREA DETECTOR |
Collection date | 1995 |
Detector | SIEMENS |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 104.000, 219.900, 86.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.000 |
R-factor | 0.187 |
Rwork | 0.187 |
R-free | 0.23300 |
RMSD bond length | 0.007 |
RMSD bond angle | 21.150 * |
Data reduction software | XENGEN |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.000 * |
Rmerge | 0.078 * |
Number of reflections | 66809 * |
Completeness [%] | 94.2 * |
Redundancy | 4.04 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | citrate | 300 (mM) | |
2 | 1 | reservoir | PEG4000 | 14 (%) |