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1FRO

HUMAN GLYOXALASE I WITH BENZYL-GLUTATHIONE INHIBITOR

Experimental procedure
Temperature [K]293
Detector technologyIMAGE PLATE
Collection date1996-02-20
DetectorRIGAKU
Spacegroup nameP 43
格子定数 [Å]68.000, 68.000, 169.400
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基7.500 - 2.200
R因子0.211
Rwork0.211
R-free0.23400
Structure solution methodMIR
結合長の平均二乗偏差(RMSD) [Å]0.009
結合角の平均二乗偏差(RMSD) [度]24.700

*

Data reduction softwareDENZO
Data scaling softwareCCP4 ((SCALA))
Phasing softwareX-PLOR
Refinement softwareX-PLOR
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)30.0002.300
分解能 [Å] (高)2.2002.200
Rmerge_l_obs0.0680.248
Total number of observations118633

*

独立反射数35503
<I/σ(I)>93
完全性 [%]91.379.1

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冗長性3.32.5
結晶化条件
結晶ID方法pH温度溶液条件
1Vapor diffusion, hanging drop

*

5.815

*

pH 5.8
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11dropPEG200012.5-15 (%(w/v))
21dropMES25 (mM)
31drop0.05 (M)
41dropprotein6 (mg/ml)
51drop2-mercaptoethanol0.5 (%)
61dropS-benzyl-glutathione1 (mM)
71reservoirPEG200025-30 (%(w/v))
81reservoirMES50 (mM)
91reservoir0.1 (M)

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件を2024-09-18に公開中

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