1FRK
AZOTOBACTER VINELANDII FERREDOXIN I: ALTERATION OF INDIVIDUAL SURFACE CHARGES AND THE [4FE-4S] CLUSTER REDUCTION POTENTIAL
Experimental procedure
Spacegroup name | P 41 21 2 |
Unit cell lengths | 55.190, 55.190, 95.390 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.100 |
R-factor | 0.227 |
Rwork | 0.227 |
RMSD bond length | 0.019 |
RMSD bond angle | 3.600 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.900 * |
Total number of observations | 50132 * |
Number of reflections | 9978 |
Completeness [%] | 83.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.4 * | 2 * | Stout, C.D., (1979) J. Biol. Chem., 254, 3598. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 7-10 (mg/ml) | |
2 | 1 | drop | potassium phosphate | 0.5 (M) | |
3 | 1 | drop | ammonium sulfate | 1.2 (M) | |
4 | 1 | reservoir | ammonium sulfate | 3.5 (M) |