1FLL
MOLECULAR BASIS FOR CD40 SIGNALING MEDIATED BY TRAF3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 108 |
Detector technology | IMAGE PLATE |
Collection date | 1999-05-27 |
Detector | MARRESEARCH |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 83.760, 83.760, 212.570 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 3.500 |
R-factor | 0.173 |
Rwork | 0.173 |
R-free | 0.31200 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.550 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.630 |
High resolution limit [Å] | 3.500 | 3.500 |
Rmerge | 0.078 | 0.260 |
Number of reflections | 29115 | |
<I/σ(I)> | 14 | |
Completeness [%] | 78.7 | 74.5 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.5 | 294 | METHANOL, SODIUM CHLORIDE, TRIS BUFFER, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |