1FLK
MOLECULAR BASIS FOR CD40 SIGNALING MEDIATED BY TRAF3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 108 |
Detector technology | IMAGE PLATE |
Collection date | 1998-05-20 |
Detector | MARRESEARCH |
Spacegroup name | H 3 |
Unit cell lengths | 84.530, 84.530, 319.500 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.800 |
R-factor | 0.224 |
Rwork | 0.224 |
R-free | 0.28600 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.890 |
High resolution limit [Å] | 2.800 | 2.790 |
Rmerge | 0.051 | 0.240 |
Number of reflections | 58040 | |
<I/σ(I)> | 18.9 | |
Completeness [%] | 98.3 | 89.1 |
Redundancy | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.5 | 294 | METHANOL, SODIUM CHLORIDE, TRIS BUFFER, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |