1FLE
CRYSTAL STRUCTURE OF ELAFIN COMPLEXED WITH PORCINE PANCREATIC ELASTASE
Experimental procedure
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1992-12-01 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.910, 73.320, 48.920 |
Unit cell angles | 90.00, 105.40, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.900 |
R-factor | 0.197 * |
Rwork | 0.197 |
RMSD bond length | 0.016 |
RMSD bond angle | 0.037 |
Data reduction software | R-AXIS |
Refinement software | PROFFT |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.900 * |
Rmerge | 0.058 |
Total number of observations | 20575 * |
Number of reflections | 15809 |
Completeness [%] | 76.8 |
Redundancy | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | macroseeding * | 5.9 | pH 5.9 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | MPD | 68-74 (%(v/v)) | |
2 | 1 | 1 | phosphate | 10 (mM) |