1FIK

HUMAN PLATELET PROFILIN I CRYSTALLIZED IN LOW SALT

Experimental procedure

Source type	ROTATING ANODE
Source details	RIGAKU RUH2R
Temperature [K]	290
Detector technology	AREA DETECTOR
Collection date	1993
Detector	SIEMENS-NICOLET X100
Spacegroup name	C 1 2 1
Unit cell lengths	74.687, 31.868, 62.425
Unit cell angles	90.00, 123.09, 90.00

Refinement procedure

Resolution	8.000 - 2.300
Rwork	0.175
Structure solution method	MIR
RMSD bond length	0.013
RMSD bond angle	0.027
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASES
Refinement software	PROFFT

Data quality characteristics

	Overall
Low resolution limit [Å]	28.400
High resolution limit [Å]	2.300
Rmerge	0.054
Number of reflections	5243
<I/σ(I)>	19.8
Completeness [%]	92.6
Redundancy	1.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		5.8		CRYSTALLIZED FROM 30% PEG 8000 SOLUTION., pH 5.8