1FIE
RECOMBINANT HUMAN COAGULATION FACTOR XIII
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-08-01 |
Detector | RIGAKU |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 101.100, 73.130, 134.700 |
Unit cell angles | 90.00, 106.40, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.500 |
R-factor | 0.182 |
Rwork | 0.182 |
RMSD bond length | 0.011 |
RMSD bond angle | 25.210 * |
Data reduction software | R-AXIS |
Data scaling software | R-AXIS |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 9999.000 * | |
High resolution limit [Å] | 2.460 * | 2.500 * |
Rmerge | 0.065 | |
Total number of observations | 101939 * | |
Number of reflections | 50732 | |
Completeness [%] | 77.7 | 62 * |
Redundancy | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 6 | pH 6. |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ethanol | 10-15 (%) | |
2 | 1 | reservoir | Tris-HCl | 0.1 (M) |