1FHM
X-RAY CRYSTAL STRUCTURE OF REDUCED RUBREDOXIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL1-5 |
Synchrotron site | SSRL |
Beamline | BL1-5 |
Temperature [K] | 103 |
Detector technology | IMAGE PLATE |
Collection date | 1999-06-28 |
Detector | FUJI |
Spacegroup name | H 3 |
Unit cell lengths | 63.355, 63.355, 32.420 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 1.500 |
RMSD bond length | 0.020 |
RMSD bond angle | 1.078 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | 10.000 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.047 | 0.047 |
Number of reflections | 9133 | |
Completeness [%] | 96.4 | 96.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 4.6 | 277 | 2M ammonium sulfate, 0.1M sodium acetate, 0.1 g sodium dithionite, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 2.0 (M) | |
2 | 1 | reservoir | sodium acetate | 0.1 (M) | |
3 | 1 | reservoir | sodium dithionite | 0.1g |