1FHG
HIGH RESOLUTION REFINEMENT OF TELOKIN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 1997-09-01 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 63.710, 63.710, 58.860 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 20.000 - 2.000 |
| R-factor | 0.233 |
| Rwork | 0.210 |
| R-free | 0.26600 |
| Structure solution method | IR |
| Starting model (for MR) | 1tlk |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.669 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.050 |
| High resolution limit [Å] | 1.980 | 1.980 |
| Rmerge | 0.070 | 0.574 |
| Number of reflections | 9904 | |
| <I/σ(I)> | 35.7 | 2.34 |
| Completeness [%] | 99.6 | 99.6 |
| Redundancy | 10.5 | 4.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4 | 273 | PEG6000, sodium acetate, pH 4.0, VAPOR DIFFUSION, SITTING DROP, temperature 273.0K |
