1FH7
CRYSTAL STRUCTURE OF THE XYLANASE CEX WITH XYLOBIOSE-DERIVED INHIBITOR DEOXYNOJIRIMYCIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | OTHER |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1999-04-01 |
Detector | MARRESEARCH |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 87.040, 87.040, 80.270 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.820 |
R-factor | 0.21 |
Rwork | 0.210 |
R-free | 0.23400 |
RMSD bond length | 0.006 |
RMSD bond angle | 22.300 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.900 |
High resolution limit [Å] | 1.820 | 1.820 |
Rmerge | 0.043 | 0.246 |
Number of reflections | 27874 | |
<I/σ(I)> | 14.7 | |
Completeness [%] | 98.6 | 97.4 |
Redundancy | 15 | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 298 | Bedarkar, S., (1992) J.Mol. Biol, 228, 693. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | Cex | 65 (mg/ml) | |
2 | 1 | drop | PEG4000 | 7.5-10 (%) | |
3 | 1 | drop | sodium acetate | 0.1 (M) | |
4 | 1 | reservoir | PEG4000 | 7.5-10 (%) | |
5 | 1 | reservoir | sodium acetate | 0.1 (M) |