1FEM
CRYSTALLOGRAPHIC STUDIES ON COMPLEXES BETWEEN RETINOIDS AND PLASMA RETINOL-BINDING PROTEIN
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.210, 48.810, 75.810 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 9.000 - 1.900 |
R-factor | 0.184 |
RMSD bond length | 0.008 * |
RMSD bond angle | 2.800 * |
Refinement software | TNT |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 9999.000 * |
High resolution limit [Å] | 1.900 * |
Rmerge | 0.105 * |
Total number of observations | 16527 * |
Number of reflections | 7294 * |
Completeness [%] | 43.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | bRBP | 6-10 (mg/ml) | |
2 | 1 | 2 | sodium chloride | 0.1 (M) | |
3 | 1 | 2 | cadmium acetate | 0.01-1. (mM) | |
4 | 1 | 2 | sodium acetate | 0.1 (M) |