1FEL
CRYSTALLOGRAPHIC STUDIES ON COMPLEXES BETWEEN RETINOIDS AND PLASMA RETINOL-BINDING PROTEIN
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.630, 49.260, 76.630 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 9.000 - 1.800 |
R-factor | 0.204 |
RMSD bond length | 0.016 * |
RMSD bond angle | 3.700 * |
Refinement software | TNT |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 9999.000 * |
High resolution limit [Å] | 1.800 * |
Rmerge | 0.062 * |
Total number of observations | 49962 * |
Number of reflections | 12128 * |
Completeness [%] | 71.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | bRBP | 6-10 (mg/ml) | |
2 | 1 | 2 | sodium chloride | 0.1 (M) | |
3 | 1 | 2 | cadmium acetate | 0.01-1. (mM) | |
4 | 1 | 2 | sodium acetate | 0.1 (M) |