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1FBM

ASSEMBLY DOMAIN OF CARTILAGE OLIGOMERIC MATRIX PROTEIN IN COMPLEX WITH ALL-TRANS RETINOL

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsELLIOTT GX-20
Temperature [K]298
Detector technologyIMAGE PLATE
Collection date1997-12-01
DetectorMARRESEARCH
Wavelength(s)1.5418
Spacegroup nameP 1 21 1
Unit cell lengths38.470, 49.470, 54.980
Unit cell angles90.00, 103.84, 90.00
Refinement procedure
Resolution3.000 - 2.700
Rwork0.195
RMSD bond length0.001
RMSD bond angle18.680

*

Data reduction softwareDENZO
Data scaling softwareCCP4 ((AGROVATA)
Phasing softwareAMoRE
Refinement softwareX-PLOR (3.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]3.0003.000
High resolution limit [Å]2.7002.700
Rmerge0.132
Total number of observations20313

*

Number of reflections5464
Completeness [%]86.087.6
Redundancy3.71
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6293COMPcc (16 mg/ml) in 20 mM sodium phosphate, 200 mM NaCl (pH 7.5) precipitant: 7-8% PEG 8000, 50 mM sodium cacodylate (pH 6.0), 50 mM sodium acetate, 50 mM calcium acetate , VAPOR DIFFUSION, HANGING DROP, temperature 20.0K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein16 (mg/ml)
21reservoirPEG80007-8 (%)
31reservoirsodium cacodylate50 (mM)
41reservoirsodium acetate50 (mM)
51reservoircalcium acetate50 (mM)

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