1FAN
CREVICE-FORMING MUTANTS IN THE RIGID CORE OF BOVINE PANCREATIC TRYPSIN INHIBITOR: CRYSTAL STRUCTURES OF F22A, Y23A, N43G, AND F45A
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.310, 23.190, 29.240 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.950 * |
R-factor | 0.169 |
Rwork | 0.169 |
RMSD bond length | 0.015 |
RMSD bond angle | 0.034 * |
Phasing software | X-PLOR |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 * |
High resolution limit [Å] | 1.950 * |
Rmerge | 0.067 * |
Total number of observations | 3493 * |
Completeness [%] | 98.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 9 * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 8 (mg/ml) | |
2 | 1 | drop | potassium phosphate | 0.6 (M) | |
3 | 1 | reservoir | potassium phosphate | 1.2-1.3 (M) |