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1F6N

CRYSTAL STRUCTURE ANALYSIS OF THE MUTANT REACTION CENTER PRO L209-> TYR FROM THE PHOTOSYNTHETIC PURPLE BACTERIUM RHODOBACTER SPHAEROIDES

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsEMBL/DESY, HAMBURG BEAMLINE BW7B
Synchrotron siteEMBL/DESY, HAMBURG
BeamlineBW7B
Temperature [K]277
Detector technologyIMAGE PLATE
Collection date1998-07-08
DetectorMARRESEARCH
Spacegroup nameP 31 2 1
Unit cell lengths141.535, 141.535, 187.913
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution50.000 - 2.800
R-factor0.221
Rwork0.221
R-free0.25100

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RMSD bond length0.010
RMSD bond angle24.100

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Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.900
High resolution limit [Å]2.8002.800
Rmerge0.0590.270
Number of reflections52164
<I/σ(I)>8.9
Completeness [%]96.095.4
Redundancy1.71.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP718

*

Fritzsch, G.,(1998) Methods Enzymol., 297, 57.

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein11 (mg/ml)
21drop4 (M)composed of 20mM NaH2PO4, 0.063%LDAO, 1.5M (NH4)2SO4, 3% 1,2,3-heptanetriol, and RC with an OD830=25.
31reservoir1.8-2.1 (M)

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