1F6B
CRYSTAL STRUCTURE OF SAR1-GDP COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 173 |
Detector technology | IMAGE PLATE |
Collection date | 1999-02-13 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.368, 61.689, 71.142 |
Unit cell angles | 90.00, 107.49, 90.00 |
Refinement procedure
Resolution | 15.000 * - 1.700 |
R-factor | 0.22 |
Rwork | 0.220 |
R-free | 0.24000 |
RMSD bond length | 0.006 * |
RMSD bond angle | 1.600 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASES |
Refinement software | CNS (0.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.000 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.050 | 0.260 |
Number of reflections | 48000 | |
<I/σ(I)> | 24.5 | |
Completeness [%] | 98.8 | 88.8 |
Redundancy | 8 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 295.5 | 30% PEG 4000, 0.2 M ammonium sulfate, and 0.1 M sodium acetate at pH 4.6, VAPOR DIFFUSION, SITTING DROP, temperature 295.5K |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 295.5 | 30% PEG 4000, 0.2 M ammonium sulfate, and 0.1 M sodium acetate at pH 4.6, VAPOR DIFFUSION, SITTING DROP, temperature 295.5K |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 295.5 | 30% PEG 4000, 0.2 M ammonium sulfate, and 0.1 M sodium acetate at pH 4.6, VAPOR DIFFUSION, SITTING DROP, temperature 295.5K |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 295.5 | 30% PEG 4000, 0.2 M ammonium sulfate, and 0.1 M sodium acetate at pH 4.6, VAPOR DIFFUSION, SITTING DROP, temperature 295.5K |