1EZ0
CRYSTAL STRUCTURE OF THE NADP+ DEPENDENT ALDEHYDE DEHYDROGENASE FROM VIBRIO HARVEYI.
Replaces: 1CO3Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X8C |
Synchrotron site | NSLS |
Beamline | X8C |
Temperature [K] | 80 |
Detector technology | AREA DETECTOR |
Collection date | 1998-03-15 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 79.380, 131.180, 92.540 |
Unit cell angles | 90.00, 92.49, 90.00 |
Refinement procedure
Resolution | 26.440 - 2.100 |
Rwork | 0.215 |
R-free | 0.24600 |
Structure solution method | MR |
Starting model (for MR) | 1eyy |
RMSD bond length | 0.006 |
RMSD bond angle | 22.500 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNS (0.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.027 | 0.051 |
Total number of observations | 189982 * | |
Number of reflections | 92467 | |
<I/σ(I)> | 24.9 | |
Completeness [%] | 83.9 | 73.7 |
Redundancy | 1.89 | 1.93 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 290 | Croteau, N., (1996) Protein Sci., 5, 2130. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 18-30 (%(w/v)) | |
2 | 1 | reservoir | sodium acetate | 200 (mM) | |
3 | 1 | reservoir | sodium cacodylate | 100 (mM) |