1EXV
HUMAN LIVER GLYCOGEN PHOSPHORYLASE A COMPLEXED WITH GLCNAC AND CP-403,700
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | OTHER |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1996-10-21 |
| Detector | MARRESEARCH |
| Spacegroup name | P 31 |
| Unit cell lengths | 124.629, 124.629, 124.064 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 99.000 - 2.400 |
| R-factor | 0.236 |
| Rwork | 0.236 |
| R-free | 0.28000 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.200 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | X-PLOR |
| Refinement software | CNS (0.5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 99.000 | 2.490 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.071 | 0.378 |
| Number of reflections | 84018 | |
| <I/σ(I)> | 19.11 | |
| Completeness [%] | 99.8 | 99 |
| Redundancy | 4.68 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 6 | 290 | MES, MPD, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 290K |
