1EWP
CRUZAIN BOUND TO MOR-LEU-HPQ
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 298 |
| Detector technology | IMAGE PLATE |
| Collection date | 1996-10-26 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.511, 51.654, 45.259 |
| Unit cell angles | 90.00, 114.76, 90.00 |
Refinement procedure
| Resolution | 25.000 - 1.750 |
| R-factor | 0.1831 |
| Rwork | 0.183 |
| R-free | 0.20600 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 2.600 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.810 |
| High resolution limit [Å] | 1.750 | 1.750 |
| Rmerge | 0.049 | 0.110 |
| Number of reflections | 17715 | |
| <I/σ(I)> | 10.8 | |
| Completeness [%] | 95.7 | 88.7 |
| Redundancy | 2.7 | 2.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 292 | 0.8M NaCitrate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 292K |
