1EWD
FRUCTOSE 1,6-BISPHOSPHATE ALDOLASE FROM RABBIT MUSCLE
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | SIEMENS |
| Temperature [K] | 298 |
| Detector technology | AREA DETECTOR |
| Collection date | 1995-11-03 |
| Detector | SIEMENS HI-STAR |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 164.194, 57.575, 85.349 |
| Unit cell angles | 90.00, 102.66, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.464 |
| Rwork | 0.170 |
| R-free | 0.23400 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.488 |
| Data reduction software | X-GEN |
| Data scaling software | X-GEN |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 |
| High resolution limit [Å] | 2.464 |
| Number of reflections | 38042 |
| Completeness [%] | 94.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | SMALL TUBES | 7.4 | 293 | Ammonium sulfate 43%, EDTA 5mM, TRIETHYLAMINE 100mM, pH 7.4, SMALL TUBES, temperature 293K |
