1EWD
FRUCTOSE 1,6-BISPHOSPHATE ALDOLASE FROM RABBIT MUSCLE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Collection date | 1995-11-03 |
Detector | SIEMENS HI-STAR |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 164.194, 57.575, 85.349 |
Unit cell angles | 90.00, 102.66, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.464 |
Rwork | 0.170 |
R-free | 0.23400 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.488 |
Data reduction software | X-GEN |
Data scaling software | X-GEN |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 |
High resolution limit [Å] | 2.464 |
Number of reflections | 38042 |
Completeness [%] | 94.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 7.4 | 293 | Ammonium sulfate 43%, EDTA 5mM, TRIETHYLAMINE 100mM, pH 7.4, SMALL TUBES, temperature 293K |