1EV1
ECHOVIRUS 1
Experimental procedure
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-13 |
Temperature [K] | 113 |
Detector technology | AREA DETECTOR |
Collection date | 1996-08 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 472.150, 483.200, 352.450 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 3.550 |
R-factor | 0.263 |
Rwork | 0.263 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | N CA AND C ATOMS FROM POLIOVIRUS |
RMSD bond length | 0.012 |
RMSD bond angle | 24.700 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.0) |
Refinement software | X-PLOR (3.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.660 |
High resolution limit [Å] | 3.550 | 3.550 |
Rmerge | 0.136 | 0.241 |
Total number of observations | 3522138 * | |
Number of reflections | 947283 | |
Completeness [%] | 97.7 | |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * | 6 * | 277 * | pH 7.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | virus | 10 (mg/ml) | |
10 | 1 | reservoir | PEG400 | 2.5 (%) | |
2 | 1 | 1 | sucrose | 30 (%) | |
3 | 1 | 1 | 1 (mM) | ||
4 | 1 | 1 | PIPES | 10 (mM) | |
5 | 1 | 1 | 25 (mM) | ||
6 | 1 | 1 | 1 (mM) | ||
7 | 1 | reservoir | PIPES | 10 (mM) | |
8 | 1 | reservoir | 25 (mM) | ||
9 | 1 | reservoir | 25 (mM) |