1EUR

SIALIDASE

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1993
Detector	SIEMENS
Spacegroup name	P 21 21 21
Unit cell lengths	48.140, 82.730, 84.750
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 1.820
R-factor	0.173
Rwork	0.173
RMSD bond length	0.016
RMSD bond angle	2.570
Data reduction software	XDS
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	1.820 *	1.820 *
Rmerge	0.055	0.094 *
Total number of observations	168296 *
Number of reflections	29469
Completeness [%]	93.4	71.7 *
Redundancy	5.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *			Taylor, G., (1992) J.Mol.Biol., 225, 1135. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG3350	8 (%)