1EUO
Crystal structure of nitrophorin 2 (prolixin-S)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS |
Temperature [K] | 298 |
Detector technology | DIFFRACTOMETER |
Collection date | 1998-10-30 |
Detector | ENRAF-NONIUS FAST |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 40.340, 127.960, 33.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 9.200 - 2.000 |
R-factor | 0.19 * |
Rwork | 0.195 |
R-free | 0.24000 * |
RMSD bond length | 0.006 * |
RMSD bond angle | 1.270 |
Data reduction software | MADNESS |
Data scaling software | SCALA |
Phasing software | X-PLOR |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 9.200 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.106 | 0.348 * |
Total number of observations | 49410 * | |
Number of reflections | 12186 | |
<I/σ(I)> | 4.5 | |
Completeness [%] | 96.9 | 90.3 |
Redundancy | 4.2 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.7 | 298 | ammonium phosphate, Tris-HCl, pH 7.7, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium phosphate | 2.8 (M) | |
2 | 1 | reservoir | Tris-HCl | 0.1 (M) |