1EQQ

SINGLE STRANDED DNA BINDING PROTEIN AND SSDNA COMPLEX

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY
Synchrotron site	Photon Factory
Temperature [K]	100
Detector technology	CCD
Collection date	1999-10-10
Detector	MARRESEARCH
Spacegroup name	C 1 2 1
Unit cell lengths	101.714, 60.473, 94.733
Unit cell angles	90.00, 112.60, 90.00

Refinement procedure

Resolution	15.000 - 3.200
R-factor	0.213
Rwork	0.213
R-free	0.33900
RMSD bond length	0.176
RMSD bond angle	3.160
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	45.000
High resolution limit [Å]	3.200
Rmerge	0.091
<I/σ(I)>	12
Completeness [%]	100.0
Redundancy	6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9	288	ammonium sulfate, pH 9.0, VAPOR DIFFUSION, HANGING DROP at 288K

Crystallization Reagents

ID	crystal ID	solution ID	reagent name	concentration	details
1	1	1	(NH4)2SO4
2	1	2	(NH4)2SO4