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1EQF

CRYSTAL STRUCTURE OF THE DOUBLE BROMODOMAIN MODULE FROM HUMAN TAFII250

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 5.0.2
Synchrotron siteALS
Beamline5.0.2
Temperature [K]100
Detector technologyCCD
Collection date1999-09-07
DetectorADSC QUANTUM 4
Spacegroup nameP 21 21 21
Unit cell lengths48.100, 58.100, 101.500
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.100 - 2.100
R-factor0.218
Rwork0.218
R-free0.24600
RMSD bond length0.009
RMSD bond angle1.140
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareMLPHARE
Refinement softwareCNS (0.9)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]51.30029.100
High resolution limit [Å]2.1002.100
Rmerge0.0790.341
Total number of observations122732

*

Number of reflections17084
<I/σ(I)>17.3
Completeness [%]97.097.6
Redundancy7.24.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1unknown

*

9.5294ammonium sulfate, TrisCl, pH 9.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
111protein10 (mg/ml)
211ammonium sulfate1.4 (M)
311Tris-HCl100 (mM)

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