1EPA

STRUCTURE OF THE EPIDIDYMAL RETINOIC ACID-BINDING PROTEIN AT 2.1 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	39.330, 58.670, 66.270
Unit cell angles	90.00, 109.34, 90.00

Refinement procedure

Resolution	6.000 - 2.100
R-factor	0.196
Rwork	0.196
RMSD bond length	0.018
RMSD bond angle	3.730
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.100 *	2.100 *
Rmerge	0.055 *
Total number of observations	63562 *
Number of reflections	16724 *
Completeness [%]	99.8 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	other *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	ammonium sulfate	40 (%sat)
2	1	1	Tris-HCl	10 (mM)
3	1	1	glycerol	10-12 (%)
4	1	1	EDTA	2.5 (mM)