1EO6
CRYSTAL STRUCTURE OF GATE-16
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2000-03-02 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.300, 76.330, 49.710 |
Unit cell angles | 90.00, 92.81, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.800 |
R-factor | 0.229 * |
Rwork | 0.229 |
R-free | 0.25600 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.220 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.060 | 0.252 |
Number of reflections | 27335 | |
<I/σ(I)> | 15.4 | |
Completeness [%] | 97.8 | 97.2 |
Redundancy | 4.2 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | PEG 8000, Tris, Calcium acetate, dimethyl sulfoxide, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | Tris | 100 (mM) | |
2 | 1 | reservoir | calcium acetate | 100 (mM) | |
3 | 1 | reservoir | PEG8000 | 22 (%) | |
4 | 1 | reservoir | 10 (%) |