1ELG

NATURE OF THE INACTIVATION OF ELASTASE BY N-PEPTIDYL-O-AROYL HYDROXYLAMINE AS A FUNCTION OF PH

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	51.080, 58.040, 75.180
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 * - 1.650
R-factor	0.17
Rwork	0.170
RMSD bond length	0.013
RMSD bond angle	2.600
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	44.000 *
High resolution limit [Å]	1.650
Number of reflections	27890 *
Completeness [%]	100.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	6.8-8.3 (mg/ml)
2	1	drop	inactivator	0.52 (mM)
3	1	drop	sodium acetate	100 (mM)
4	1	reservoir	sodium sulphate	100 (mM)
5	1	reservoir	acetate	100 (mM)