1EJX
CRYSTAL STRUCTURE OF WILD-TYPE KLEBSIELLA AEROGENES UREASE AT 100K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | FUJI |
Spacegroup name | I 21 3 |
Unit cell lengths | 168.960, 168.960, 168.960 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.600 |
Rwork | 0.172 |
R-free | 0.24000 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.107 | 0.314 |
Number of reflections | 97194 | |
Completeness [%] | 93.0 | 93 |
Redundancy | 4.3 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | lithium sulfate, Hepes, EDTA, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |