1EET

HIV-1 REVERSE TRANSCRIPTASE IN COMPLEX WITH THE INHIBITOR MSC204

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	LURE BEAMLINE D41A
Synchrotron site	LURE
Beamline	D41A
Temperature [K]	279
Detector technology	IMAGE PLATE
Collection date	1997-07-09
Detector	MARRESEARCH
Spacegroup name	C 2 2 21
Unit cell lengths	119.570, 156.450, 156.350
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.500 - 2.730
R-factor	0.213
Rwork	0.213
R-free	0.27100
RMSD bond length	0.007
RMSD bond angle	1.400
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	X-PLOR
Refinement software	CNS (0.9)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.500	2.900
High resolution limit [Å]	2.730	2.730
Rmerge	0.102	0.558
Number of reflections	36910
<I/σ(I)>	7.2
Completeness [%]	94.1	88.4
Redundancy	1.9	1.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.2	294	This particular structure is not described in this paper. *