1EDN
HUMAN ENDOTHELIN-1
Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1992-11-12 |
| Detector | MARRESEARCH |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 33.350, 33.350, 59.280 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 2.180 |
| R-factor | 0.199 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 3.960 |
| Data reduction software | MOSFLM |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 8.000 |
| High resolution limit [Å] | 2.180 |
| Rmerge | 0.107 |
| Total number of observations | 8907 * |
| Number of reflections | 1876 |
| Completeness [%] | 99.0 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | X-ray capillaries * |
